Performance Qualification (PQ) of Weighing Balance in Pharma Industry

 

Performance Qualification (PQ) of Weighing Balance in Pharma Industry

In the pharmaceutical industry, weighing balances play a critical role in ensuring accuracy and compliance during manufacturing and quality control processes. To maintain data integrity and regulatory compliance, balances must undergo qualification as per Good Manufacturing Practices (GMP). After IQ (Installation Qualification) and OQ (Operational Qualification), the final stage is PQ – Performance Qualification.

PQ verifies that the balance performs consistently and accurately under actual working conditions. Let’s explore how to perform PQ for a weighing balance.

What is Performance Qualification (PQ)?

Performance Qualification is the documented evidence that a weighing balance operates consistently and delivers accurate results during routine usage. PQ ensures that the balance is reliable not just in theory, but also in the real working environment.

Steps to Perform PQ for Weighing Balance

1. Preparation

Identify the balance (ID, model, capacity).

Ensure the environment is stable (no vibration, no air flow, proper temperature).

Use calibrated, certified standard weights (E2/F1 class as per balance resolution).

2. Repeatability Test

Place the same standard weight (e.g., 10 g) on the pan 10 times.

Record each reading.

Calculate the Standard Deviation (SD) and %RSD.

Acceptance: %RSD should meet balance specification (e.g., ≤0.1%).

3. Linearity Test

Use at least 5 different standard weights across the balance range (e.g., 10 g, 50 g, 100 g, 200 g).

Compare observed vs. actual values.

Acceptance: Deviation must be within ±0.1% or as per SOP.

4. Accuracy Test

Check low, medium, and high capacity weights.

Readings should be within acceptance tolerance.

5. Eccentricity (Corner Load) Test

Place a standard weight at the center and at four corners of the pan.

Variation between positions should not exceed defined limits.

Documentation

All results must be documented in the PQ report. Include:

Test method and procedure

Observed readings

Calculations (SD, %RSD, deviations)

Acceptance criteria comparison

Conclusion (Pass/Fail)

Example Acceptance Criteria

Repeatability: %RSD ≤ 0.1%

Linearity: Deviation within ±0.1%

Accuracy: ± tolerance per SOP

Eccentricity: Within manufacturer’s limits

Conclusion

Performance Qualification (PQ) of a weighing balance ensures the instrument is accurate, reliable, and compliant under routine conditions. It safeguards product quality, regulatory compliance, and patient safety. By performing PQ at defined intervals (e.g., annually) or after major maintenance, organizations can maintain confidence in their weighing processes.

👉 A well-documented PQ not only fulfills GMP requirements but also strengthens the company’s quality assurance system.

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